IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

Marihuana Potency Analysis by
High Performance Liquid Chromatography

Testing Accreditation #: 77802 Test Certificate #: 144984-001
Client Name, Sample Details

Bloominati Farms LLC (AU-G-C-001217)
Warren, MI 48089
Sample: Papaya Bomb
License: AU-G-C-001217
Type: Adult Use Flower
Method: FE04U12 HPLC-UV
Metrc Test Pkg#: 1A405030003FB25000000119
Metrc Source Pkg#: 1A405030003FB25000000116
***Water Activity: 0.51

Test Conditions

Prepsheet ID#: MIP240117a
Scale: XS205-MI2
Temp: 22.9 °C
Baro Pressure: 976.9 hPa
Analyst: MEH
Technician: ARH

Sample ID#: 144984

Harvest/Process Date: 01/16/2024
Serving Size (g): 1
Date Received: 01/16/2024
Test Date: 01/17/2024
Valid Through: 01/17/2025
Report Issued: 01/19/2024

Sample #144984
Sample #144984 Sample #144984
Test
Compounds
Δ9-THC THCA Δ8-THC CBD CBDA CBG CBGA CBN CBC CBL THCV CBDV Total
Cannabinoids*
Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 0.9 25.7 N/D N/D N/D 0.1 0.6 N/D N/D N/D N/D N/D 27.3 23.4 0.0 24.1
Amount (mg/g) 8.9 256.5 N/D N/D N/D 1.1 6.44 N/D N/D N/D N/D N/D 272.94 233.9 0.0 240.6
Amount per Serving (mg) 8.9 256.5 N/D N/D N/D 1.1 6.44 N/D N/D N/D N/D N/D 272.9 Serving Size~ (g): 1.0
LOQ (mg/g) 0.79 0.79 0.79 0.79 0.79 0.79 0.79 0.79 0.79 0.79 0.79 0.79   %Decarb. THC CBD
±%RPD 1.82% 0.18% 0.99% 0.73% 0.42% 0.20% 0.43% 0.10% 0.46% 2.47% 0.50% 3.78% 3 N/A

Sample passes for water activity (sample fails if Aw>0.65).

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009.

FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products.

Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of Δ9-THC and Δ8-THC or CBD plus the amount of THC or CBD derived from THCA or CBDA, respectively.

These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value.

Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, Total CBG, CBC, THCV, CBDV, and CBL.

Total CBG is calculated as CBG plus CBGA*0.878 (the molar correction factor for CBGA to CBG conversion).

%Decarb. THC and CBD refer to the percentage of Δ9-THC or CBD relative to THCA or CBDA, respectively.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

ARH - LM Iron laboratories ARH - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

QC Report

Testing Accreditation #: 77802 Test Certificate #: 144984-001
Client Name, Sample Details

Bloominati Farms LLC (AU-G-C-001217)
Warren, MI 48089
Sample: Papaya Bomb
License: AU-G-C-001217
Type: Adult Use Flower
Method: FE04U12 HPLC-UV
Metrc Test Pkg#: 1A405030003FB25000000119
Metrc Source Pkg#: 1A405030003FB25000000116
***Water Activity: 0.51

Test Conditions

Prepsheet ID#: MIP240117a
Scale: XS205-MI2
Temp: 22.9 °C
Baro Pressure: 976.9 hPa
Analyst: MEH
Technician: ARH

Sample ID#: 144984

Harvest/Process Date: 01/16/2024
Serving Size (g): 1
Date Received: 01/16/2024
Test Date: 01/17/2024
Valid Through: 01/17/2025
Report Issued: 01/19/2024

Sample #144984
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Δ9-THC 0 5.88905 5.67902 96.43 5.57675 94.70 1.82%
THCA 0 5.42864 5.45276 100.44 5.46281 100.63 0.18%
Δ8-THC 0 5.86972 5.63739 96.04 5.58191 95.10 0.99%
CBD 0 5.74229 5.82841 101.50 5.87134 102.25 0.73%
CBDA 0 5.47405 5.50836 100.63 5.48514 100.20 0.42%
CBG 0 5.64477 5.77711 102.34 5.76549 102.14 0.20%
CBGA 0 5.32901 5.42859 101.87 5.40517 101.43 0.43%
CBN 0 5.62352 5.62031 99.94 5.61445 99.84 0.10%
CBC 0 5.51706 5.56112 100.80 5.58658 101.26 0.46%
CBCA 0 0 0 0.00 0 0.00 0%
CBL 0 5.47365 5.55503 101.49 5.69405 104.03 2.47%
THCV 0 5.55509 5.51822 99.34 5.49056 98.84 0.50%
CBDV 0 5.6697 5.59805 98.74 5.81378 102.54 3.78%

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

ARH - LM Iron laboratories ARH - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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