IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

Marihuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 77802 Test Certificate #: 142268-001
Client Name, Sample Details

The Brand Labs (Pinebrook) Warren LLC AU-P-000198
Warren, MI 48092
Sample: Grape Zaza
License: AU-P-000198
Type: AU Vape Cart
Method: FE04U12 HPLC-UV
Metrc Test Pkg#: 1A4050300021D69000103195
Metrc Source Pkg#: 1A4050300021D69000103192
Test Conditions

Prepsheet ID#: MIP230914A
Scale: XS205-MI2
Temp: 21.5 °C
Baro Pressure: 987.1 hPa
Analyst: SKM
Technician: SKM
Sample ID#: 142268

Harvest/Process Date: 09/13/2023
Serving Size (g): 1
Date Received: 09/13/2023
Test Date: 09/14/2023
Valid Through: 09/14/2024
Report Issued: 09/15/2023
Sample #142268
Sample #142268 Sample #142268
Test
Compounds		 Δ9-THC THCA Δ8-THC CBD CBDA CBG CBGA CBN CBC CBL THCV CBDV Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 80.9 N/D N/D 0.3 N/D 2.0 N/D 1.7 1.3 N/D 0.8 N/D 87.0 80.9 0.3 87.0
Amount (mg/g) 809.1 N/D N/D 3.0 N/D 20.0 N/D 17.0 12.8 N/D 7.6 N/D 869.5 809.1 3.0 869.5
Amount per Serving (mg) 809.1 N/D N/D 3 N/D 20 N/D 17 12.8 N/D 7.6 N/D 869.5 Serving Size~ (g): 1.0
LOQ (mg/g) 2.61 2.61 2.61 2.61 2.61 2.61 2.61 2.61 2.61 2.61 2.61 2.61   %Decarb. THC CBD
±%RPD 0.74% 0.29% 0.29% 0.01% 0.87% 0.83% 1.85% 0.14% 0.55% 0.64% 0.53% 0.12% 100% 100%

Sample tested for potency and vitamin E acetate. Sample does not contain vitamin E acetate over 100 ug/g (PASS).

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009.

FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products.

Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of Δ9-THC and Δ8-THC or CBD plus the amount of THC or CBD derived from THCA or CBDA, respectively.

These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value.

Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, Total CBG, CBC, THCV, CBDV, and CBL.

Total CBG is calculated as CBG plus CBGA*0.878 (the molar correction factor for CBGA to CBG conversion).

%Decarb. THC and CBD refer to the percentage of Δ9-THC or CBD relative to THCA or CBDA, respectively.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
ARH - LM Iron laboratories ARH - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

QC Report
Testing Accreditation #: 77802 Test Certificate #: 142268-001
Client Name, Sample Details

The Brand Labs (Pinebrook) Warren LLC AU-P-000198
Warren, MI 48092
Sample: Grape Zaza
License: AU-P-000198
Type: AU Vape Cart
Method: FE04U12 HPLC-UV
Metrc Test Pkg#: 1A4050300021D69000103195
Metrc Source Pkg#: 1A4050300021D69000103192
Test Conditions

Prepsheet ID#: MIP230914A
Scale: XS205-MI2
Temp: 21.5 °C
Baro Pressure: 987.1 hPa
Analyst: SKM
Technician: SKM
Sample ID#: 142268

Harvest/Process Date: 09/13/2023
Serving Size (g): 1
Date Received: 09/13/2023
Test Date: 09/14/2023
Valid Through: 09/14/2024
Report Issued: 09/15/2023
Sample #142268
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Δ9-THC 0 5.22893 5.23988 100.21 5.20113 99.47 0.74%
THCA 0 5.04438 5.08671 100.84 5.07174 100.54 0.29%
Δ8-THC 0 5.15239 5.28257 102.53 5.26712 102.23 0.29%
CBD 0 5.49871 5.25156 95.51 5.25112 95.50 0.01%
CBDA 0 5.2014 5.12881 98.60 5.17355 99.46 0.87%
CBG 0 5.32503 5.23564 98.32 5.27921 99.14 0.83%
CBGA 0 4.97216 4.97039 99.96 5.06296 101.83 1.85%
CBN 0 5.13726 5.16974 100.63 5.16251 100.49 0.14%
CBC 0 5.0428 5.06775 100.49 5.03993 99.94 0.55%
CBCA 0 0 0.00 0 0.00 0%
CBL 0 4.87923 5.13103 105.16 5.16402 105.84 0.64%
THCV 0 5.22192 5.21229 99.82 5.24011 100.35 0.53%
CBDV 0 5.172 5.21775 100.88 5.22376 101.00 0.12%

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
ARH - LM Iron laboratories ARH - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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